Autosampler Vials and Caps for HPLC, LC-MS, GC, and GC-MS. Thermo Scientific vials and closures are available in a wide range of options to fit every HPLC, GC, and MS instrument—as well as your application and budget. Thermo Scientific Autosampler Compatibility Chart (PDF, 192 KB) Performance Level 1: Everyday Analysis
Feb 9, 2023 · 1. Proper Storage: Chromatography vials should be stored in a cool, dry place away from light and moisture. Vials should also be stored away from sources of contamination such as chemicals
Chromatography Vials. With thousands of combinations to choose from, DWK Life Sciences offers the largest and most diverse selection of chromatography lab vial solutions and microplates. Our ISO 9001 facility manufactures vials that meet or exceed OEM specifications for headspace, routine HPLC/GC use, plus Certified vials for LCMS/GCMS.
2 Our portfolio includes over 850 Thermo Scientific vials and closures products designed for any instrument and any application. Our pages have been arranged by product line and vial size, allowing you to quickly find the most appropriate products for your lab. Featured Products Sample Handling Products SureStop 9mm Vials
May 30, 2023 · Accurate and consistent vial filling is critical to reliable analysis. Filtration techniques like pipetting or automated filling systems should be utilized to ensure the appropriate amount of sample is added into each vial; overfilling or underfilling can result in inaccurate results, so precise measurements must be maintained at all times.
HPLC & GC Certified Screw Vial & Cap Kits for 2 mL Samples. Precleaned, EPA certified assembled kits; includes 40 mL screw vials and 24 mm. open top screw caps. 0.3 and 1.5 mL screw top vial-cap kits for analysis of small sample volumes. For use with environmental analyses under EPA regulations.
In this application brief, Waters provides a short list of best practices to characterize oligonucleotides by ion-pair reversed-phase (IP-RP) liquid chromatography. These best practices cover column selection, separation temperature, pH optimization, pore size selection, mobile phase choice, rapid method development considerations, purification
The FIRST and ONLY pre-cleaned, low particle, low background chromatography vial When your instrumentation, sample handling and methodology is pushing the limits, a chromatography vial that can keep up is essential. • The only chromatography vials pre-cleaned to provide unmatched consistency • The ˜ rst low particle, low background
Best Practices - Technical Note 3 How to prepare samples • Filtering through 0.2 µm filters is the preferred method to remove the insoluble fraction from samples and avoid blockages in the system. If not possible, centrifuge samples vigorously and be careful not to contaminate the supernatant with precipitates while decanting or aspirating it.
Jun 22, 2020 · The sample handling and preparation stages are particularly important when either the sample volume is limited or when detecting and quantifying analytes present at low concentrations. The quality of glass vials that these samples are prepared and stored in, a commonly overlooked factor, can have a major impact on the results.
Jul 29, 2022 · Flush with 5 column volumes of a mobile phase without buffers to remove any buffers or salts. Store the column in 65% acetonitrile/35% water. Cleaning (if high backpressure is observed): Rinse with 10 column volumes each of: 95% water/5% acetonitrile (for buffer removal) THF. 95% water/5% acetonitrile. Mobile phase.
Injection Volume: 30 μL Sample: 1. Caffeine 2. Salicylamide A. Injection Solvent 100% Acetonitrile B. Injection Solvent Mobile Phase Tip: Injecting in a solvent stronger than the mobile phase can cause peak shape problems such as peak splitting or broadening Trick: Keep Organic Concentration in Sample Solvent < Mobile Phase
COE is a result of the concentration of Boric Acid in the borosilicate glass used to manufacture a vial, and the chemical resistance properties of the glass. Clear borosilicate glass with a COE of 33 or 51, and amber borosilicate glass with a COE of 51 are known as Type 1. They deliver the best overall vial performance, with: • Lower pH shifts
Robotic Arm Machines (R.A.M.) use a non-standard 9mm vial with a magnetic cap. For autosamplers, choose a vial designed for that specific brand. Inserts can be used to decrease the capacity of the vial while maintaining the exterior dimensions. They are useful for smaller samples to ensure the correct amount of sample is aspirated from the vial.
Jun 16, 2021 · Defining sample preparation. While sample handling describes the processes of collection and transport, sample preparation focusses on the techniques used to improve analytical results. Before undergoing analysis, researchers may use techniques such as Solid-Phase Extraction and Gravimetric Sample Preparation to “clean up” a sample and