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Mar 10, 2022 · An Overview of High Recovery Vials. High recovery vials have a total capacity of about 1.5mL, but the tapered conical finish of the vial bottom allows for the needle to be able to draw up the last few microliters. If you are looking for a high recovery vial, or any other autosampler vial to use in your workflow, contact Chrom Tech today for a
Fisherbrand™ Glass Autosampler Vial Inserts. Fisherbrand™ glass autosampler vial inserts are available in precision point and flat bottom profiles and are compatible with 9 mm HPLC and GC autosampler vials. Height (Metric) 31 mm. Diameter (Metric) Outer.
Purge pump at high flow rate (e.g., 5-10 mL/min.), prime system if necessary. (Prime each pump head separately.) If system has check valve, loosen valve to allow air to escape. If problem persists, flush system with 100% methanol or isopropanol. If problem still persists, contact system manufacturer.
solution in water/acetonitrile (98/2; v/v). Seven dilutions of the stock solution are prepared, leading to calibration solutions containing 20, 4, 0.8, 0.16, 0.032, 0.006, and 0.001 µg/mL caffeine. Calibration is performed in the range of 0.006 to 20 µg/mL. The 0.006 µg/mL calibration solution is further diluted for
Just as in GC applications, patterns in your HPLC chromatography can exhibit telltale signs that point toward probable sources of error. In this brief series of posts, we will look at possible scenarios that you may encounter in the laboratory and how you might approach resolving those difficulties.
9mm screw thread vials have a standard 12x32 profile compatible with most autosamplers Microsampling vials allow for max sample extraction without separate inserts High recovery vials combine large sample capacities with near full sample extraction Manufactured from clear, Type 1 Class A
Aijiren's autosampler vials include a wide range of HPLC vials and GC vials designed and optimized to work with Aijiren autosamplers & HPLC, GC platforms. These HPLC and GC vials are available as snap, screw or crimp in style, 15uL to 20 mL in sample size, and various of low bleed and high-quality material composition.
HTA offers different solutions for Liquid Chromatography (HPLC, UHPLC, NanoLC, Preparative LC, FPLC, LC-MS) as listed below. Our solutions can be easily installed on all kinds of analyzers by a quick and trouble-free installation. Visit the product pages to discover how you can improve your analysis.
Often the easiest first step is to try a manual injection valve or to replace the autosampler with one that has not been exposed to the compound of interest. If either of these approaches correct the problem, it confirms that the problem is in the autosampler and further troubleshooting efforts along this line are worthwhile.
The autosampler component of a HPLC system is used to increase sample throughput, improve the precision of injections, and allow for unattended operation. Its main components are a needle or syringe, a metering device to measure sample volume, and a sample loop.
Dec 20, 2021 · ANSWER. The syringe needle of an autosampler does not go all the way to the bottom of a vial, so some sample always remains. This is referred to as the "residual volume" of the vial. Some vials have a tapered bottom, which decreases the residual volume. This can be important if the sample is valuable or if only a small amount is available.
An available dual split sampler is designed for use with the Thermo Scientific Vanquish Duo UHPLC system for Dual LC workflows. Offering reliability, excellent peak shape, and efficient separations, Thermo Scientific UltiMate 3000 autosamplers support a variety of sample formats and a range of pressures up to 1000 bar.
1-4mL Autosampler Vials for HPLC, UPLC, GC 16mm, 25mm Test Tubes for Water Analysis especially when high protein recovery is desired. Hamag Lab Use Syringe Filter ...
Dec 12, 2012 · Recoveries from UPLC System. Sample solutions prepared by water:methanol as the diluent were placed into the autosampler for evaluation. The sample withdrawing speeds were selected at the default setting of 100 μL/minute and two other slower speeds of 50 μL/minute and 20 μL/minute.
Fisherbrand™ Glass Autosampler Vial Inserts Fisherbrand™ glass autosampler vial inserts are available in precision point and flat bottom profiles and are compatible with 9 mm HPLC and GC autosampler vials. 2 Fisherbrand™ 150 μL Spring Insert